Steaming
of ErtelAlsop Lenticular Pak®
Depth Filters
Please read the following
instructions in their entirety prior to
performing the procedure.
Installation
Filter housings must be cleaned
prior to installation of filter cartridges to remove any residual contaminant,
including residues from prior use. This includes but is not limited
to O-ring grooves and O-rings and threads. Refer to your in-house validated
cleaning procedures.
A vent valve should be installed
at the top of the housing in order to expel air at the start of steaming
and during introduction of the process liquid.
A pressure gauge for monitoring
steam pressure should be installed on the filter assembly.
Steam Requirement
Steam should be free from
particulate such as rust and scale from piping. An appropriate steam
filter, such as porous stainless steel cartridges should be used or
the steam source should be a clean steam generator.
Use dry and saturated steam.
Do not use superheated steam.
Minimum steam conditions
are 15 psig (121o C) and maximum steam conditions are 25 psig (130o
C).
Caution
ErtelAlsop lenticular Pak® cartridges are designed to withstand differential pressures up to 30
psig at 80oC in the forward direction and limited back pressure. Excessive
reverse pressure can damage the cartridge. This procedure is designed
to avoid this condition.
Only clean, oil free air
or nitrogen should be used.
If water hammer from cycling
valves or hydrostatic downstream head are present, appropriate protection
should be provided to prevent back flow or hydraulic shock which can
damage the filter.
Pulsating flow to the filter
should be avoided.
Steaming
This procedure is designed
for in-line steaming of the lenticular Pak® filter assembly. Contact
ErtelAlsop for information about steam autoclaving the Pak® filter
or filter assembly.
Refer to the diagram in Figure 1.
1. Air/nitrogen (D) and steam
inlet valve (A) should be closed.
2. Close the inlet valve
(B) and filter outlet valve (G).
3. Fully open the filter
outlet valve (F).
4. Crack open valve (H) and
the filter housing vent (E) and drain valves (I, J).
5. Open the steam inlet valve
(A) and valve (C).
6. Fully close the filter
housing vent (E) valve as soon as steam flow is apparent.
CAUTION: Valves will
be hot and could cause injury if touched without appropriate protection.
Exposure to the steam
flow from the vent valve (E) may cause injury. Direct the flow with
appropriate tubing such that contact with personnel is avoided.
7. Steam flow through the
filter assembly should proceed for 30 minutes or as long as experience
dictates.
Monitor steam pressure via
the pressure gauge on the filter housing making sure that pressure does
not fall below 15 psig. A pressure gauge may be installed immediately
downstream of the filter assembly to monitor differential pressure across
the filter cartridge.
8. Close the steam inlet
valve (A) and drain valve (H).
9. Close valve (C). In order
to avoid excessive back pressure, clean oil free air or nitrogen may
be introduced to the upstream side of the filter assembly when the steam
pressure falls below 15 psig through air/nitrogen valve (D).
10. Air/nitrogen should be
regulated to 15 psig. Open valve (D).
11. Immediately close valve
(I) and drain valve (J).
12. Close air/nitrogen valve
(D).
13. Allow the filter assembly
to cool to ambient temperature.
This procedure is represented as being typical and is based on experience
in our laboratories. It may not be representative of your specific physical
arrangements or validated standard operating procedures. Please contact
ErtelAlsop if you have any questions.